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World Journal of Pharmacy and
Pharmaceutical Sciences

( An ISO 9001:2015 Certified International Journal )

An International Peer Reviewed Journal for Pharmaceutical and Medical Research and Technology

Impact Factor : 8.485

ICV : 84.65

WJPPS Citation

	All	Since 2020
Citation	6651	4087
h-index	26	21
i10-index	174	83

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Abstract

DEVELOPMENT AND VALIDATION OF AN RP-HPLC METHOD FOR ANALYSIS OF CRISABOROLE

Amol Pimpale*, Sheetal Gondkar and Smita Aher

ABSTRACT

A simple, sensitive and accurate RP-HPLC method has been developed for the determination of Crisaborole in bulk formulation. The λmax of the Crisaborole was found to be 241nm in 10 mM Ammonium acetate buffer: ACN [60:40 % v/v]. pH 4.5. The method shows high sensitivity with linearity 5 to 25μg/ml (regression equation: y = 316606x - 427583; r2 = 0.9992). The various parameters according to ICH guidelines and USP are followed for validating and testing of this method. The Detection limit and quantitation limit were found to be 0.1094 μg ml –1 and 0.3316 μg ml–1 respectively. The results demonstrated that the procedure is accurate, specific and reproducible (RSD

Keywords: Crisaborole, HPLC method.

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